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Advance Battery Failure Analysis and Materials Optimization while Preserving Sample Integrity 

Advance Battery Failure Analysis and Materials Optimization while Preserving Sample Integrity. 

 

Tescan solutions

for advanced research in batteries
Production and Quality Assurance

Achieve consistent quality in lithium-ion battery manufacturing while preserving sensitive cell structures. Tescan FIB-SEM and micro-CT workflows deliver reproducible 2D and 3D insights essential for battery quality assurance, covering electrodes, powders, separators, and full cells.

Tomography and automated SEM analysis highlight porosity, particle variation, and separator morphology, while non-destructive CT supports battery diagnostics by revealing electrode alignment and anode overhang in assembled cells.

Enable reliable results that improve yield, validate processes, and accelerate decision-making across the battery lifecycle.

Production and Quality Assurance
Failure Analysis

Understand battery failure analysis under real-world conditions without disrupting fragile internal structures. Tescan FIB-SEM and micro-CT workflows provide multimodal insight into thermal effects, electrode damage, and hidden defects linked to battery degradation mechanisms.

In-situ heating and electrolyte visualization reveal gas formation and chemical shifts in real time, while 3D tomography supports battery post-mortem analysis by capturing particle fracturing, delamination, and lithium trapping within electrodes.

Deliver reliable results that strengthen safety testing, inform root cause analysis, and extend battery lifespan.

Failure Analysis
Raw Materials Optimization

Improve battery performance consistency by ensuring the quality of lithium, nickel, cobalt, and graphite feedstocks. Tescan’s automated mineralogy workflows provide high-throughput characterization to evaluate deposits, refine beneficiation, and reduce variability in electrode manufacturing.

With Tescan TIMA, complex ores are mapped to distinguish similar phases, quantify liberation and grain size, and model associations critical for recovery. These insights support efficient resource use, strengthen battery material analysis, and create more reliable supply chains for lithium-ion production.

Deliver reliable results that improve process control, support battery validation, and optimize raw material utilization across the energy storage lifecycle.

Raw Materials Optimization
Recycling

Support sustainable battery production by maximizing recovery of critical materials from spent cells. Tescans automated mineralogy workflows deliver particle-level insight into complex black mass mixtures, helping recyclers refine processes, optimize battery recycling workflows, and improve yields.

Tescan TIMA classifies each particle by chemistry and morphology—distinguishing cathode chemistries, quantifying liberation, and identifying graphite, foils, and alloys. These insights refine recovery strategies, reduce waste, and support battery upcycling initiatives.

Deliver reliable results that strengthen circular economy goals, improve process efficiency, and secure a consistent supply of recovered materials for lithium-ion production.

Recycling
Research and Development

Advance battery innovation with workflows that capture processes from nanoscale chemistry to full-cell structures. Tescan imaging and analysis solutions reveal interfaces, visualize dynamics, and map phases with clarity—supporting safer, longer-lasting, and higher-performing designs.

FIB-SEM with ToF-SIMS exposes electrode formation and solid-state interfaces, while 4D-STEM resolves crystallographic phases and strain at the nanometer scale. In-situ micro-CT complements these insights by tracking electrolyte movement and thermal effects in intact cells.

Deliver reliable results that accelerate material discovery, guide cell design, and shape the next generation of battery technologies.

TS_Section_3D Characterization

Pioneering Successes

in Battery Development

“At Dragonfly Energy, our goal is to deliver a more sustainable and cost-effective Li-ion battery, and these metrics are fundamentally defined by dynamic nanoscale interactions occurring inside the cell. TESCAN’s electron microscopy and micro-CT solutions provide valuable, correlative insights into the behavior of these complex systems which enable the development of our innovative cell chemistries.”


DR. DENIS PHARES 

CEO at Dragonfly Energy

 

Quote-Denis-Phares

Tescan Instruments & Technology

Used in This Workflow
MICRO_UniTOM_XL_1-1

Tescan UniTOM XL Micro-CT

Engineered for non-destructive 3D imaging, UniTOM XL delivers high-resolution scans of complete lithium-ion cells, components, and modules.

  • Large-format micro-CT: Image cylindrical, pouch, and prismatic batteries without disassembly
  • Sub-micron voxel resolution: Capture fine electrode geometry, tabs, and separators in full 3D
  • Dynamic & in-situ capability: Visualize heating, cooling, electrolyte dynamics, and gas formation in real time
  • Compatible with VGSTUDIO MAX & Panthera™: Advanced segmentation, analysis, and digital twin integration
AMBER-X2

Tescan AMBER X Plasma FIB-SEM 

Built for advanced battery and materials research, AMBER X integrates plasma FIB milling with ultra-high-resolution SEM imaging.

  • High-current Xe plasma FIB: Section large battery electrodes or multilayer stacks quickly and cleanly
  • Correlative multimodal analysis: Combine structural imaging with STEM, R-STEM, and EDS in one workflow
  • Plasma FIB-SEM for large volumes: Ideal for porosity mapping, electrode degradation, and 3D reconstruction
  • Field-free SEM imaging: Achieve high-contrast, low-kV imaging for delicate battery features
CLARA GM Mat. Science

Tescan AMBER X 2 Plasma FIB-SEM 

A next-generation FIB-SEM platform optimized for high-throughput and correlative battery analysis.

  • Multimodal integration: Plasma FIB with SEM, STEM, R-STEM, and ToF-SIMS modules
  • High-throughput milling: Enables large-area lamella prep and 3D cross-sectional analysis of electrode stacks
  • Inert transfer compatibility: Maintain sample integrity from glovebox to microscope
  • Tailored for degradation studies: Visualize SEI morphology, interfacial failure, and elemental depth profiles
TIMA GM

 Tescan CLARA UHR SEM 

Ultra-high-resolution SEM tailored for nanostructure and surface characterization.

  • True UHR SEM imaging: Resolve nanopores and fiber networks in separators and electrode coatings
  • Essence™ software automation: Automate particle sizing, morphology, and statistical analysis of powders
  • Non-destructive workflows: Analyze separator porosity and coating uniformity at the nanoscale
  • Stable low-voltage imaging: Ideal for beam-sensitive battery materials
MICRO_UniTOM_HR_1-1

Tescan TIMA – Automated Mineralogy Platform 

Purpose-built for raw material optimization and recycling, TIMA delivers automated mineralogy at particle scale.

  • Automated EDS-based mineral identification: Map lithium-bearing phases like spodumene, lepidolite, and amblygonite
  • Particle-based analysis: Assess grain size, liberation, and mineral associations for process optimization
  • Integrated workflows: Supports upstream resource modeling and downstream black mass recycling
  • Quantitative deportment analysis: Track lithium, cobalt, and nickel across size fractions

Tescan PolyDET II Spectral Detector 

An advanced spectral detection module for UniTOM XL, enabling material separation and chemical imaging.

  • Spectral CT capability: Differentiate materials based on X-ray absorption spectra
  • Elemental mapping: Visualize distribution of heavy vs. light elements in electrodes and casings
  • Non-destructive: Analyze internal defects and compositional variation in sealed cells
  • High sensitivity: Supports advanced R&D and QA workflows in battery development

Tescan ToF-SIMS Module 

Integrated within Tescan FIB-SEM platforms, ToF-SIMS provides high-sensitivity surface and interface chemistry mapping.

  • Lithium and electrolyte mapping: Track elemental and isotopic distributions across electrode interfaces
  • 2D and 3D depth profiling: Reveal chemical gradients through SEI or solid-state interfaces
  • Correlative with SEM/FIB: Align chemical and structural data in one dataset
  • Essential for solid-state research: Study adhesion, ion mobility, and interface degradation

Tescan RSTEM (Rotational STEM) 

An integrated STEM mode within AMBER X 2 for nanometer-scale subsurface analysis.

  • Rotational STEM imaging: Enhance contrast and resolution for thin lamella characterization
  • Nanostructural analysis: Visualize SEI layering, intergranular cracking, and cathode degradation
  • Correlative with FIB prep: Prepare lamella and analyze nanoscale details in one workflow
  • Ideal for advanced failure studies: Detect atomic-scale degradation mechanisms in electrodes

Tescan Essence™ Software


A modern SEM workflow automation platform that simplifies complex analyses.

  • Automated particle analysis: Generate size, morphology, and distribution data for powders
  • Intuitive interface: Streamline image acquisition and reporting with minimal training
  • Integrated statistics: Produce reliable datasets for QC and R&D labs
  • Scalable workflows: Move seamlessly from R&D to production environments

Tescan Acquila™ Software + In-Situ Heating Stage 

A dynamic CT acquisition platform integrated with UniTOM XL for thermal experiments.

  • In-situ heating integration: Perform controlled heating and cooling of cells during scanning
  • Scriptable acquisition: Automate temperature protocols and time-lapse imaging sequences
  • Real-time visualization: Track electrolyte movement, gas pocket formation, and structural changes
  • Advanced experimental flexibility: Combine mechanical, thermal, and dynamic CT in one setup

Explore the system that
moves your research
forward

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